HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 136029342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | 2-Ethyl-5-(4-(tritylthio)phenyl)-1,3,4-oxadiazole | HCID 68488331 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 136029342 | HCID 136029342 | — |
Reaction Steps
2-Ethyl-5-(4-(tritylthio)phenyl)-1,3,4-oxadiazole was dissolved in trifluoroacetic acid (5 ml) and a large excess of triethyl silane (500 μl) was added. The solution was stirred for 10 minutes then the solvent was removed under a stream of nitrogen to leave 4-(5-ethyl-1,3,4-oxadiazol-2-yl)benzenethiol-Compound F 98 mg (99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288536B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-3b29c06771ee43a1b5005e6147c1b392 |
| Source note | uspto-grants-2012_10 |