HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluorotryptophan → HCID 45254376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluorotryptophan | HCID 9577 | — |
| Reactant | 2,6-Dichloroquinoline-3-carboxylic acid | HCID 24266068 | — |
| Product | HCID 45254376 | HCID 45254376 | 90% |
Reaction Steps
In close analogy to the procedure described in Example 1, 2,6-dichloroquinoline-3-carboxylic acid is reacted with 5-fluoro-DL-tryptophan to provide the title compound in 90% yield as yellow needles (recrystallization from DMF/water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288549B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-99bfacef8ad247d69704961b82cfd225 |
| Source note | uspto-grants-2012_10 |