HCID 178499428, compound → HCID 178513299, compound

Participants

Reaction Steps

A solution of methyl [4-(N-hydroxycarbamimidoyl)-phenyl]-acetate (3.67 g, 17.6 mmol) in 25% aq. HCl (15 mL) is stirred at 65° C. for 4 h. The solvent is removed in vacuo and the residue is dried under high vacuum to give [4-(N-hydroxycarbamimidoyl)-phenyl]-acetic acid (3.80 g, presumably as hydrochloride) as a yellow solid; LC-MS: tR=0.34 min, [M+1]+=195.05.

Provenance & Evidence