Propanal → HCID 67214298, compound

HRID 2065989Notes

Reaction equation

HRID 2065989 reaction equation
[ClH:1].[CH:2]1[C:15]2[NH:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[CH:5]=[CH:4][C:3]=1[C:16]1[N:17]=[C:18]([CH2:21][NH2:22])[S:19][CH:20]=1.[CH:23](=O)[CH2:24][CH2:25][CH2:26][CH3:27].C(=O)CC>>[ClH:1].[CH:2]1[C:15]2[NH:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[CH:5]=[CH:4][C:3]=1[C:16]1[N:17]=[C:18]([CH2:21][NH:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[S:19][CH:20]=1

Participants

4

Reactant 3

HCID 527PropanalHCID 8063PentanalHCID 67213853HCID 67213853, compound

Product 1

HCID 67214298HCID 67214298, compoundYield 38%

Procedure

The experimental protocol used is the same as that described for Stage 399.1 of Example 399, with the compound of Example 362 and valeraldehyde replacing intermediate 355.2 and propionaldehyde respectively. A dark-coloured solid is obtained with a yield of 38%. MH+=382.2.

Workup

  1. customA dark-coloured solid is obtained with a yield of 38%

Sources & evidence

ORD record
ord-5f149642428242cc9523e078d97203a5
Source dataset
uspto-grants-2012_10
Patent number
US08288560B2

Reaction notes

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