Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | L-Phenylalanine | HCID 6140 | — |
| Reactant | Butyric anhydride | HCID 7798 | — |
| Product | Phenylalanine butyramide | HCID 68631493 | — |
Reaction Steps
5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08293253B2 |
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| Source dataset | uspto-grants-2012_10 |
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| ORD ID | ord-75a29ee0177b41b9a5c82eed28243734 |
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| Source note | uspto-grants-2012_10 |
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