3-Aminophenol → HCID 836761, compound

HRID 2066384Notes

Reaction equation

[NH2:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.[CH:9]1([C:14](Cl)=[O:15])[CH2:13][CH2:12][CH2:11][CH2:10]1>>[OH:8][C:4]1[CH:3]=[C:2]([NH:1][C:14]([CH:9]2[CH2:13][CH2:12][CH2:11][CH2:10]2)=[O:15])[CH:7]=[CH:6][CH:5]=1

Participants

Reactant 2

HCID 115683-Aminophenol

HCID 78284Cyclopentanecarbonyl chloride

Product 1

HCID 836761HCID 836761, compoundYield 56.5%

Procedure

By using 3-aminophenol (1.0 g) and cyclopentanecarbonyl chloride (607 mg) as starting materials, the title compound (531 mg) was obtained in the same manner as that of Reference Example 18.

Sources & evidence

ORD record: ord-8c5205a4b2a84f23a275317651f1a691
Source dataset: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08293715B2

Reaction notes

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