HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxyacetophenone → HCID 67388732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxyacetophenone | HCID 8487 | — |
| Reactant | HCID 178424304 | HCID 178424304 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67388732 | HCID 67388732 | — |
Reaction Steps
By using 3′-hydroxyacetophenone (200 mg) and a 1 M solution of o-tolylmagnesium chloride in tetrahydrofuran (4.4 ml) as starting materials, the title compound (119.3 mg) was obtained in the same manner as that of Reference Example 69.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293715B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-cf92cdbcf99641db98642483d456c092 |
| Source note | uspto-grants-2012_10 |