m-Tolyl isocyanate → HCID 66681599, compound

HRID 2066428Notes

Reaction equation

HRID 2066428 reaction equation
[N:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[CH:5]=1)=[C:2]=[O:3].[CH3:11][C:12]1([CH3:26])[C:16]([CH3:18])([CH3:17])[O:15][B:14]([C:19]2[CH:25]=[CH:24][C:22](N)=[CH:21][CH:20]=2)[O:13]1.FC1C=CC=C([N:34]=C=O)C=1>>[CH3:11][C:12]1([CH3:26])[C:16]([CH3:18])([CH3:17])[O:15][B:14]([C:19]2[CH:25]=[C:24]([NH:34][C:2]([NH:1][C:4]3[CH:5]=[C:6]([CH3:10])[CH:7]=[CH:8][CH:9]=3)=[O:3])[CH:22]=[CH:21][CH:20]=2)[O:13]1

Participants

4

Reactant 3

HCID 69303m-Tolyl isocyanateHCID 1230643-Fluorophenyl isocyanateHCID 27346204-(Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Product 1

HCID 66681599HCID 66681599, compound

Procedure

The title compound was prepared by substituting 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline and 1-isocyanato-3-methylbenzene for 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline and 1-fluoro-3-isocyanatobenzene, respectively in Example 1D.

Sources & evidence

ORD record
ord-61e5bf6b658a418dbc4181c5555b514b
Source dataset
uspto-grants-2012_10
Patent number
US08293738B2

Reaction notes

Loading…