HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-5-fluoro-2-methyl-3-nitrobenzene → 4-Bromo-6-fluoro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-5-fluoro-2-methyl-3-nitrobenzene | HCID 2773385 | — |
| Reactant | 4-bromo-1H-indole-6-sulfonic acid dimethylamide | HCID 59151342 | — |
| Product | 4-Bromo-6-fluoro-1H-indole | HCID 24728173 | — |
Reaction Steps
Prepared according to the method used in the preparation of 4-bromo-1H-indole-6-sulfonic acid dimethylamide using 1-bromo-5-fluoro-2-methyl-3-nitro-benzene in place of 3-bromo-4-N,N-trimethyl-5-nitro-benzenesulfonamide. The title compound was obtained as a white solid (6.06 g, 33%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293735B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-fc678e33e145496ba290d55824f81a21 |
| Source note | uspto-grants-2012_10 |