HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 86649581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 58095730 | HCID 58095730 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86649581 | HCID 86649581 | — |
Reaction Steps
CDI (0.13 g) was added to a stirred solution of 4′-methyl-2-(1-trifluoromethyl-cyclopropyl)-[4,5]bithiazolyl-2′-ylamine (Step 10.2) (0.16 g) in CH2Cl2 (5 mL) at rt. The reaction mixture was then stood for 3 h at 25° C. and the title compound isolated by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293753B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-dbc65e0e25174d29bdec4357ce778c8c |
| Source note | uspto-grants-2012_10 |