HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 178446220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 178446210 | HCID 178446210 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 178446220 | HCID 178446220 | — |
Reaction Steps
The title compound was prepared by reacting 6-bromo-1-(pentan-3-yl)-1H-imidazo[4,5-b]pyrazin-2-ol (1.0 equiv), sodium thiomethoxide (1.4 equiv), and N-methylpyrrolidone (5.9 volume equivalents) in a manner analagous to Example 1(c). LCMS m/z (APCI)=253.0 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293761B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-353506399c3d4715962ab81a8613637c |
| Source note | uspto-grants-2012_10 |