HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 68664078, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 69077070 | HCID 69077070 | — |
| Product | HCID 68664078 | HCID 68664078 | — |
Reaction Steps
A mixture of 387 mg of so obtained 2-(2-benzyloxycarbonyl-aminoethyl)-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylic acid and 4.5 mL of hydrobromic acid was stirred at room temperature for 3 hours, and thereafter the solvent was distilled off under reduced pressure to provide 410 mg (quantitative) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293754B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-3c56ca27bfdc47a4be52e8b0a3534bc1 |
| Source note | uspto-grants-2012_10 |