HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178499180, compound → HCID 178499176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178499180 | HCID 178499180 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178499176 | HCID 178499176 | — |
Reaction Steps
A mixture of 4-nitro-1H-pyrazole-3-carboxylic acid methyl ester (34.6 mmol) and 10% Pd/C (650 mg) in EtOH (150 ml) is stirred under an atmosphere of hydrogen for 20 hours. The mixture is filtered through a plug of Celite, reduced in vacuo and dried through azeotrope with toluene to afford 4-amino-1H-pyrazole-3-carboxylic acid methyl ester
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293767B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-ca2d6d2efa0f438cbeab64814fb75efc |
| Source note | uspto-grants-2012_10 |