Propionic Acid → HCID 86625665, compound

HRID 2067150Notes

Reaction equation

HRID 2067150 reaction equation
[C:1]([OH:5])(=[O:4])[CH2:2][CH3:3].[C:6]([O-:10])(=[O:9])[CH2:7][CH3:8].[Na+:11]>>[C:1]([O-:5])(=[O:4])[CH2:2][CH3:3].[C:6]([O-:10])(=[O:9])[CH2:7][CH3:8].[C:1]([O-:5])(=[O:4])[CH2:2][CH3:3].[Na+:11].[Na+:11].[Na+:11]

Participants

3

Reactant 2

HCID 1032Propionic AcidHCID 2723816Sodium Propionate

Product 1

HCID 86625665HCID 86625665, compound

Conditions

Temperature
70 °C

Procedure

555 g of propionic acid and 350 g of sodium propionate were added to a 0.5 l stirred vessel equipped with jacket bottom outlet valve, anchor agitator and cryostat and heated to 70° C. until a homogeneous melt was obtained. The melt was drained off into a metal shell and set on cooling. The resultant solid (858 g) which was comminuted and dried for 6 h at 45° C. under a water-jet vacuum had a propionic acid content of 61.64% by weight and a water content of 0.08% by weight.

Workup

  1. customequipped with jacket bottom outlet valve
  2. customwas obtained
  3. temperatureon cooling
  4. customdried for 6 h at 45° C. under a water-jet vacuum

Sources & evidence

ORD record
ord-20ea9dd0cdfc4afdb2d2f9d1716cf738
Source dataset
uspto-grants-2012_10
Patent number
US08293793B2

Reaction notes

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