HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11577394, compound → HCID 11633801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11577394 | HCID 11577394 | — |
| Reactant | HCID 11612479 | HCID 11612479 | — |
| Product | HCID 11633801 | HCID 11633801 | — |
Reaction Steps
The reaction was carried out similarly as described in the preparation of compound 102, using compound 121 (1.63 mmol). The crude product was purified by continuous gradient flash chromatography using EtOAc/petroleum ether (40-60) 50:50 to 100:0 as the eluent to afford the title compound as yellow syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293772B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-060a10055dab4aa9a2192df2b6f74f24 |
| Source note | uspto-grants-2012_10 |