2,3-Dichloroaniline → HCID 11706040, compound

Participants

Reaction Steps

The reaction was carried out similarly as described in the preparation of compound 148, using compound 471 (0.13 mmol) and 2,3-dichloro-phenylamine (0.13 mmol). The crude product was purified by flash chromatography using MeOH/DCM 1:20 as the eluent to afford the title compound. 13C NMR (CDCl3) δ 194.9, 146.4, 140.4, 139.1, 138.5, 135.1, 134.8, 134.0, 133.5, 132.7, 130.0, 127.6, 124.3, 123.2, 122.5, 121.0, 119.9, 118.6, 117.4, 115.2, 61.5, 28.7, 20.1

Provenance & Evidence