HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluoroaniline → HCID 11641326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluoroaniline | HCID 96595 | — |
| Reactant | HCID 11510648 | HCID 11510648 | — |
| Reactant | HCID 69606498 | HCID 69606498 | — |
| Product | HCID 11641326 | HCID 11641326 | — |
Reaction Steps
The reaction was carried out similarly as described in the preparation of compound 148, using compound 471 (0.13 mmol) and 3,5-difluoro-phenylamine (0.13 mmol). The crude product was purified by flash chromatography using MeOH/DCM 1:20 as the eluent to afford the title compound. 13C NMR (CDCl3) δ 195.0, 163.8 (dd), 146.6, 146.4, 143.1 (t), 140.5, 138.4, 135.2, 134.8, 133.6, 132.7, 132.6, 132.3, 129.4, 122.5, 121.0, 120.1, 118.1, 114.5, 102.2 (m), 98.2 (t), 61.5, 28.8, 20.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293772B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-ce77a9a10a3e49349982152346b8b983 |
| Source note | uspto-grants-2012_10 |