Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium Succinate | HCID 9020 | — |
| Reactant | Ethanol sodium succinate | HCID 86659235 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Succinic Acid | HCID 1110 | — |
| Product | Sodium Sulfate | HCID 24436 | — |
Reaction Steps
A mixture of 32.06 g of 200 proof ethanol and 4.325 g of 98% sodium succinate was prepared and heated to 30° C. H2SO4 (2.5386 g, 98%) was then added to the ethanol/sodium succinate slurry while stirring to produce free succinic acid and sodium sulfate. Following the procedure described in Example 1, a conversion of 86.6% of sodium succinate was obtained after 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08293935B2 |
|---|
| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-d36f28e5c76441a4a517423731bd2a21 |
|---|
| Source note | uspto-grants-2012_10 |
|---|
