HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 2-Dodecylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 1-Dodecene | HCID 8183 | — |
| Product | 2-Dodecylphenol | HCID 171144 | 59.9% |
Reaction Steps
First, dodecyl phenol was prepared. Specifically, to a 2-liter four-necked flask, 325 g of phenol and 30 g of dried activated clay (manufactured by MIZUSAWA INDUSTRIAL CHEMICALS, LTD.: product name, Galeonite #136) were added. 575 g of 1-dodecene was dropped in this mixture with agitation at 135 degrees C. for 4 hours. The activated clay was filtered, and then 537 g of dodecyl phenol was obtained by vacuum distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299004B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-a47df7d20255403da9929f3bf66de330 |
| Source note | uspto-grants-2012_10 |