HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(4-Bromophenyl)prop-2-enoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p-Bromocinnamic acid | HCID 99777 | — |
| Product | 3-(4-Bromophenyl)prop-2-enoyl chloride | HCID 53411293 | — |
Reaction Steps
A solution of compound 2 (113.8 g, 0.5 mol) in thionyl chloride was refluxed for 1.5 h. Then the mixture was concentrated in vacuo and the crude product 3 was obtained (126.9 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299023B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-07ed3d842a034ae78d9fc7a652770e7e |
| Source note | uspto-grants-2012_10 |