HuagongsheHuagongshe Chemistry Print Report · For research reference only
phenylalaninol, (R)- → HCID 69338592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | phenylalaninol, (R)- | HCID 853475 | — |
| Reactant | N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide | HCID 58964482 | — |
| Product | HCID 69338592 | HCID 69338592 | 65% |
Reaction Steps
N-(6-Fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide (30 mg, 0.0943 mmol) is reacted with (R)-2-amino-3-phenyl-propan-1-ol according to the GPA affording 22.2 mg (65%) of a purple powder. Rt=4.40 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299085B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-8912953b472c4990984275ebe70468f2 |
| Source note | uspto-grants-2012_10 |