(4-Chlorophenoxy)acetic acid → (4-Chlorobenzyloxy)acetic acid

HRID 2069327Notes

Reaction equation

HRID 2069327 reaction equation
ClC1C=CC([O:6][CH2:7][C:8]([OH:10])=[O:9])=CC=1.[Cl:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18]Br)=[CH:16][CH:15]=1>>[Cl:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18][O:6][CH2:7][C:8]([OH:10])=[O:9])=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 26229(4-Chlorophenoxy)acetic acidHCID 693291-(Bromomethyl)-4-chlorobenzene

Product 1

HCID 352006(4-Chlorobenzyloxy)acetic acid

Procedure

(4-Chlorobenzyloxy)acetic acid was prepared in analogy to (4-chlorophenoxy)-acetic acid using 4-chlorobenzyl bromide as precursor. The product with the molecular weight of 200.62 (C9H9ClO3) was obtained in this way; MS (ESI): 222.95 (M+Na—H).

Workup

  1. customThe product with the molecular weight of 200.62 (C9H9ClO3) was obtained in this way

Sources & evidence

ORD record
ord-b51aafa3feb948fb8ed84debab544d9a
Source dataset
uspto-grants-2012_10
Patent number
US08299104B2

Reaction notes

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