HCID 66933549, compound → HCID 66933444, compound

HRID 2069387Notes

Reaction equation

HRID 2069387 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[C:10]([CH2:12][CH3:13])[N:9]=[C:8]([S:14]([CH3:17])(=[O:16])=[O:15])[N:7]=1)=[O:5])[CH3:2].[CH2:18](OC(C1C=C(CCC)N=C(SC)N=1)=O)C>>[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[C:10]([CH2:12][CH2:13][CH3:18])[N:9]=[C:8]([S:14]([CH3:17])(=[O:16])=[O:15])[N:7]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 66933549HCID 66933549, compoundHCID 66933557HCID 66933557, compound

Product 1

HCID 66933444HCID 66933444, compound

Procedure

The title compound is obtained as a yellow solid (107 mg) in analogy to 6-ethyl-2-methanesulfonyl-pyrimidine-4-carboxylic acid ethyl ester starting from 2-methylsulfanyl-6-propyl-pyrimidine-4-carboxylic acid ethyl ester; LC-MS: tR=0.85 min, [M+H]+=272.96.

Sources & evidence

ORD record
ord-86362590f59642f8a9779bf2bc008c00
Source dataset
uspto-grants-2012_10
Patent number
US08299086B2

Reaction notes

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