HCID 54759244, compound → HCID 54759243, compound

HRID 2069388Notes

Reaction equation

HRID 2069388 reaction equation
[CH2:1]([C:3]1[N:8]=[C:7]([S:9]([CH3:12])(=[O:11])=[O:10])[N:6]=[C:5]([C:13]([OH:15])=[O:14])[CH:4]=1)[CH3:2].[CH2:16](OC(C1C=C(CCC)N=C(SC)N=1)=O)C>>[CH3:12][S:9]([C:7]1[N:6]=[C:5]([C:13]([OH:15])=[O:14])[CH:4]=[C:3]([CH2:1][CH2:2][CH3:16])[N:8]=1)(=[O:11])=[O:10]

Participants

3

Reactant 2

HCID 54759244HCID 54759244, compoundHCID 66933557HCID 66933557, compound

Product 1

HCID 54759243HCID 54759243, compound

Procedure

The title compound is obtained as a yellow solid (371 mg) in analogy to 6-ethyl-2-methanesulfonyl-pyrimidine-4-carboxylic acid starting from 2-methylsulfanyl-6-propyl-pyrimidine-4-carboxylic acid ethyl ester; LC-MS: tR=0.65 min, [M+H]+=244.95.

Sources & evidence

ORD record
ord-4ee50d77b87a4c4b9265d1a7a2a886f6
Source dataset
uspto-grants-2012_10
Patent number
US08299086B2

Reaction notes

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