HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 59216455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Fluoro-1-indanone | HCID 136537 | — |
| Reactant | Azetidine hydrochloride | HCID 12308726 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 59216455 | HCID 59216455 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
5-fluoro-1-indanone (7.44 g, 49.5 mmol), Azetidine HCl (5.1 g, 54.4 mmol) and K2CO3 (13.6 g, 99 mmol) were taken up in 60 ml of DMSO. The reaction mixture was heated at 100° C. for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299077B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-6b5c96058666464db6324fd1de31ffce |
| Source note | uspto-grants-2012_10 |