Methanesulfonic Acid → HCID 59216517, compound

Participants

Reaction Conditions

Reaction Steps

5-azetidin-1-yl-indan-1-one (1.9 g, 10.14 mmol) and methane sulfonic acid (10.8 ml) were added to CH2Cl2 (100 ml). The reaction mixture was cooled to 0° C. and sodium azide (1.32 g, 20.29 mmol) was carefully portion wise added over 30 min then reaction mixture was stirred at 0° C. for 2 hours. After the reaction was done, it was slowly added 20% NaOH aq. at 0° C.

Provenance & Evidence