HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178488270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl xanthate | HCID 8823 | — |
| Reactant | 2-Amino-4-methoxyphenol | HCID 1419108 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178488270 | HCID 178488270 | — |
Reaction Steps
The mixture containing 2-amino-4-methoxyphenol (1 eq) and O-ethylxanthic acid, potassium salt (1.1 eq) in pyridine was refluxed for two hours. The resultant mixture was poured in to ice/water containing hydrochloric acid to yield a 5-methoxybenzoxazole-2-thiol as a tan solid. MS: MH+=182
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299108B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-af1050922e9c40c98bfd9f7aa8e93878 |
| Source note | uspto-grants-2012_10 |