HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → Methyl 5-bromo-4-methyl-1H-pyrrole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl 4-methyl-1H-pyrrole-3-carboxylate | HCID 15274278 | — |
| Product | Methyl 5-bromo-4-methyl-1H-pyrrole-3-carboxylate | HCID 66924763 | — |
Reaction Steps
By a similar operation as in Reference Example 22 and using methyl 4-methyl-1H-pyrrole-3-carboxylate (1.0 g) and N-bromosuccinimide (1.28 g), the title compound was obtained as a pale-yellow solid (yield 489 mg, 31%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299261B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-db0a8a8201474ada9e08cb0a901295ad |
| Source note | uspto-grants-2012_10 |