3-Cyano-5-isopentylpyridine → methyl 3-(aminomethyl)-5-(N-methylmethylsulfonamido)benzoate

HRID 2070960Notes

Reaction equation

HRID 2070960 reaction equation
[N:1]([CH2:4][C:5]1[CH:6]=[C:7]([CH:12]=[C:13]([N:15]([CH3:20])[S:16]([CH3:19])(=[O:18])=[O:17])[CH:14]=1)[C:8]([O:10][CH3:11])=[O:9])=[N+]=[N-].C(C1C=NC=C(CCC(C)C)C=1)#N>>[NH2:1][CH2:4][C:5]1[CH:6]=[C:7]([CH:12]=[C:13]([N:15]([CH3:20])[S:16]([CH3:19])(=[O:18])=[O:17])[CH:14]=1)[C:8]([O:10][CH3:11])=[O:9]

Participants

3

Reactant 2

HCID 686702083-Cyano-5-isopentylpyridineHCID 86647414methyl 3-(azidomethyl)-5-(N-methylmethylsulfonamido)benzoate

Product 1

HCID 59570003methyl 3-(aminomethyl)-5-(N-methylmethylsulfonamido)benzoate

Procedure

The desired product was synthesized from methyl 3-(azidomethyl)-5-(N-methylmethylsulfonamido)benzoate following the general procedure as described for 3-cyano-5-isopentylpyridine.

Sources & evidence

ORD record
ord-4afc6510d58046ec8d8e36eb111148e2
Source dataset
uspto-grants-2012_10
Patent number
US08299267B2

Reaction notes

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