N-Methylmethanesulfonamide → HCID 59569821, compound

HRID 2071060Notes

Reaction equation

HRID 2071060 reaction equation
[CH:1]([C:4]1[CH:5]=[C:6]([CH:16]=[C:17]([CH2:19][NH:20][S:21]([CH3:24])(=[O:23])=[O:22])[CH:18]=1)[CH2:7][NH:8]C(=O)OC(C)(C)C)([CH3:3])[CH3:2].CNS(C)(=O)=O>>[NH2:8][CH2:7][C:6]1[CH:16]=[C:17]([CH:18]=[C:4]([CH:1]([CH3:3])[CH3:2])[CH:5]=1)[CH2:19][NH:20][S:21]([CH3:24])(=[O:23])=[O:22]

Participants

3

Reactant 2

HCID 97632N-MethylmethanesulfonamideHCID 68671471HCID 68671471, compound

Product 1

HCID 59569821HCID 59569821, compound

Procedure

N-(3-(aminomethyl)-5-isopropylbenzyl)methanesulfonamide was synthesized from the tert-butyl 3-isopropyl-5-(methylsulfonamidomethyl)benzylcarbamate following the general procedure as described above for the N-methyl methylsulfonamide.

Sources & evidence

ORD record
ord-f4c950aceded4007ab89d1a9571ae49f
Source dataset
uspto-grants-2012_10
Patent number
US08299267B2

Reaction notes

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