3-ButenaMide, 3-Methyl- → HCID 86647431, compound

HRID 2071063Notes

Reaction equation

HRID 2071063 reaction equation
BrC1C=C(C=C(S(ONC)(=O)=O)C=1)C#N.[CH3:16][NH:17][O:18][S:19]([C:22]1[CH:23]=[C:24]([CH:27]=[C:28]([C:30]([CH3:32])=[CH2:31])[CH:29]=1)[C:25]#[N:26])(=[O:21])=[O:20].C(CC(N)=O)(C)=C>>[CH3:16][NH:17][O:18][S:19]([C:22]1[CH:23]=[C:24]([CH:27]=[C:28]([C:30]([CH3:32])=[CH2:31])[CH:29]=1)[C:25]#[N:26])(=[O:21])=[O:20].[CH:30]([C:28]1[CH:27]=[C:24]([CH:23]=[C:22]([S:19]([O:18][NH:17][CH3:16])(=[O:21])=[O:20])[CH:29]=1)[C:25]#[N:26])([CH3:32])[CH3:31]

Participants

5

Reactant 3

HCID 102407683-ButenaMide, 3-Methyl-HCID 86647429HCID 86647429, compoundHCID 86647431HCID 86647431, compound

Product 2

HCID 86647431HCID 86647431, compoundHCID 86647432HCID 86647432, compound

Procedure

3-(methylaminooxysulfonyl)-5-(prop-1-en-2-yl)benzonitrile was synthesized from the 3-bromo-5-(methylaminooxysulfonyl)benzonitrile following the general procedure as described herein for the chloro substituted pyridine. 3-isopropyl-5-(methylaminooxysulfonyl)benzonitrile was synthesized from 3-(methylaminooxysulfonyl)-5-(prop-1-en-2-yl)benzonitrile following the general procedure as described herein for the isopropenyl acetamide.

Sources & evidence

ORD record
ord-e113430e7aed40ae8106abaa8c58e3e9
Source dataset
uspto-grants-2012_10
Patent number
US08299267B2

Reaction notes

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