HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Azidomethyl)benzofuran → 2-(Aminomethyl)benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Azidomethyl)benzofuran | HCID 86647433 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(Aminomethyl)benzofuran | HCID 19079348 | — |
Reaction Steps
A mixture of 2-(azidomethyl)benzofuran and 267 mg of 20% Pd(OH)2 in 10 mL of MeOH was stirred at r.t. under H2 balloon for 2.5 h. The mixture was filtered through Celite and concentrated to give the crude benzofuran-2-ylmethanamine which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299267B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-dfb824ff00a045259c508633e6f36e4f |
| Source note | uspto-grants-2012_10 |