HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21413051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 2306203 | HCID 2306203 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21413051 | HCID 21413051 | — |
Reaction Steps
A solution of 19.3 g. of 2-phenylhydrazino-2-thiazoline in 200 ml. of dry ethyl ether and 50 ml. of methanol is saturated with dry hydrogen chloride gas at 0° C. and stored at 0°-5° C. for 4 days. The crystalline material is filtered and washed with ether affording 16.5 g. of 2-phenylhydrazino-2-thiazoline hydrochloride, m.p. 300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046753 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-5231f6d34f7148bb9aa84bfdead736f7 |
| Source note | uspto-grants-1977_09 |