HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → 3,5-Dinitro-4-[2-methoxyethyl-amino]-2-chlorobenzotrifluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 2,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene | HCID 94398 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | 3,5-Dinitro-4-[2-methoxyethyl-amino]-2-chlorobenzotrifluoride | HCID 20571868 | — |
Reaction Steps
The compound was prepared by reacting 2-methoxyethylamine with 2,4-dichloro-3,5-dinitrobenzotrifluoride in cyclohexane to give the product melting at 106.5°-107.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046758 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-31af9a257813437caadd7812fa238df8 |
| Source note | uspto-grants-1977_09 |