HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 88826767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1,2-Ethanedisulfonic Acid | HCID 8032 | — |
| Reactant | 4-Methoxy-2-methyl-5-(methylsulfanyl)pyridin-3-ol | HCID 69710 | — |
| Product | HCID 88826767 | HCID 88826767 | — |
Reaction Steps
A mixture of 9.25 gm. (0.05 m) 5-mercaptopyridoxine, 4.75 gm. (0.025 m) of ethane-1,2-disulfonic acid, and 40 ml. of water is heated briefly until solution occurs. The solution is cooled and the precipitate collected by filtration. Recrystallization from methanol gives bis(2-methyl-3-hydroxy-4-hydroxymethyl-5-mercaptomethylpyridinium) ethane-1,2-disulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046897 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-dd466e7485f04a509ffe2ee1593a19eb |
| Source note | uspto-grants-1977_09 |