HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Piperidone → HCID 22754294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Piperidone | HCID 12665 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | Phenoxazine | HCID 67278 | — |
| Product | HCID 22754294 | HCID 22754294 | — |
Reaction Steps
Reaction of phenoxazine, 2-piperidone, and phosphorus oxychloride according to the procedure of Example 1 provides 10-(3,4,5,6-TETRAHYDRO-2-PYRIDYL)PHENOXAZINE HYDROCHLORIDE, m.p. 218.5°-221° C. (corr.), in a 27% overall yield from absolute ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046891 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-0a82f513458c4258a1331deee5f3adb4 |
| Source note | uspto-grants-1977_09 |