HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 1-Nitro-2-methylamino-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1-(Methylsulfanyl)-2-nitro-N-(2-{[(1,3-thiazol-2-yl)methyl]sulfanyl}ethyl)ethen-1-amine | HCID 70542948 | — |
| Product | 1-Nitro-2-methylamino-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene | HCID 70541840 | — |
Reaction Steps
Reaction of 1-nitro-2-methylthio-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene with methylamine according to the process of Example 8(ii) yielded the title compound, m.p. 103°-104°. (from ethanol ether). (Found: C, 39.4; H, 5.2; N, 20.2% C9H14N4O2S2 requires: C, 39.4; H, 5.1; N, 20.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046907 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-d1191a52964e4e84828d68bf0697ad45 |
| Source note | uspto-grants-1977_09 |