Ethylamine → 1-Nitro-2-ethylamino-2-[2-((2-amino-5-1,3,4-thiadiazolyl)methylthio)ethylamino]ethylene

HRID 2071468Notes

Reaction equation

HRID 2071468 reaction equation
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[S:15][C:14]([NH2:16])=[N:13][N:12]=1)([O-:3])=[O:2].[CH2:19]([NH2:21])[CH3:20]>>[N+:1]([CH:4]=[C:5]([NH:21][CH2:19][CH3:20])[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[S:15][C:14]([NH2:16])=[N:13][N:12]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 6341EthylamineHCID 705428991-Nitro-2-methylthio-2-[2-((2-amino-5-1,3,4-thiadiazolyl)methylthio)ethylamino]ethylene

Product 1

HCID 705434241-Nitro-2-ethylamino-2-[2-((2-amino-5-1,3,4-thiadiazolyl)methylthio)ethylamino]ethylene

Procedure

Reaction of 1-nitro-2-methylthio-2-[2-((2-amino-5-(1,3,4)-thiadiazolyl)methylthio)ethylamino]ethylene (see Example 85(i)) with ethylamine by the procedure of Example 8(ii) gives the title product.

Sources & evidence

ORD record
ord-3de49f49430b42f988febbd9d41ca050
Source dataset
uspto-grants-1977_09
Patent number
US04046907

Reaction notes

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