HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Fluorotoluene → HCID 20311720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Fluorotoluene | HCID 9606 | — |
| Reactant | 1-Acetylpiperidine-4-carbonyl chloride | HCID 100950 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 20311720 | HCID 20311720 | — |
Reaction Steps
By following the manipulative procedure described above in Example 4(a), 25 g of 1-acetylisonipecotoyl chloride are added to stirred suspension of 25 g of aluminum chloride and 14 g of m-fluorotoluene in 220 ml of ethylene dichloride to produce the oil, 1-acetyl-4-(2-fluoro-4methylbenzoyl)piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046900 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-77bf6802cc944486bfe214f76e13d948 |
| Source note | uspto-grants-1977_09 |