HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine N-Oxide → HCID 178473426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine N-Oxide | HCID 12753 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 20331700 | HCID 20331700 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178473426 | HCID 178473426 | 62% |
Reaction Steps
The procedure of Example 3 was repeated except that Step 2 relating to the oxidation to the pyridine-oxide was changed, whereby a chloroform solution of 2-ethoxycarbonylamino-6-bromopyridine was treated with m-chloroperbenzoic acid as the oxidizing agent for 9 days at room temperature, giving a 62% yield of 2-ethoxycarbonylamino-6-bromopyridine-1-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04048181 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-a24a6b88468e4285b85426d973c2bf92 |
| Source note | uspto-grants-1977_09 |