5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene → HCID 21412102, compound

HRID 2071731Notes

Reaction equation

HRID 2071731 reaction equation
[CH2:1]([N:8]([CH2:11][CH2:12][CH2:13][CH:14]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[CH:18]=[CH:17][C:16]2[CH:25]=[CH:26][CH:27]=[CH:28][C:15]1=2)CC)[C:2]1C=CC=CC=1>[Pd]>[CH2:1]([NH:8][CH2:11][CH2:12][CH2:13][CH:14]1[C:15]2[CH:28]=[CH:27][CH:26]=[CH:25][C:16]=2[CH:17]=[CH:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]1=2)[CH3:2]

Participants

3

Reactant 1

HCID 214121395-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene

Product 1

HCID 21412102HCID 21412102, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

5-[3-(N-Benzyl-N-ethylamino)-propyl]-5H-dibenzo[a,d]cycloheptene is dissolved in absolute alcohol and hydrogenated over palladium on alumina catalyst at 40°-60° C. The catalyst is separated and the product isolated by evaporating the solvent.

Workup

  1. customThe catalyst is separated
  2. customthe product isolated
  3. customby evaporating the solvent

Sources & evidence

ORD record
ord-092666f5cfdc4233a8628ffd02e08cc8
Source dataset
uspto-grants-1977_09
Patent number
US04048223

Reaction notes

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