HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 6-Methoxy-2-naphthylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Methyl 6-methoxynaphthalene-2-acetate | HCID 90324 | — |
| Solvent | Water | HCID 962 | — |
| Product | 6-Methoxy-2-naphthylacetic acid | HCID 32176 | — |
Reaction Steps
A mixture of 25 g. of methyl 6-methoxy-2-naphthylacetate, 15 g. of sodium carbonate, 200 ml. of methanol, and 25 ml. of water are stirred for 24 hours. The reaction mixture is then acidified with 200 ml. of 2 N hydrochloric acid and extracted with methylene chloride. The extracts are combined, washed with water, dried over sodium sulfate, and evaporated to yield 6-methoxy-2-naphthylacetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04048330 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-56af59978731472ea9e897d7c3bc05f1 |
| Source note | uspto-grants-1977_09 |