2,2,4,4-Tetramethyl-1,3-cyclobutanedione → HCID 21412707, compound

HRID 2071865Notes

Reaction equation

[C:1]([NH:5][NH2:6])([CH3:4])([CH3:3])[CH3:2].[CH3:7][C:8]1([CH3:16])[C:11](=[O:12])[C:10]([CH3:14])([CH3:13])[C:9]1=O>>[C:1]([NH:5][N:6]=[C:9]1[C:8]([CH3:16])([CH3:7])[C:11](=[O:12])[C:10]1([CH3:14])[CH3:13])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 136172,2,4,4-Tetramethyl-1,3-cyclobutanedione

HCID 81890tert-Butylhydrazine

Product 1

HCID 21412707HCID 21412707, compound

Procedure

2,2,4,4-Tetramethylcyclobutan-1,3-dione mono-t-butylhydrazone was prepared by refluxing an aqueous solution of t-butylhydrazine with an equimolar amount of 2,2,4,4-tetramethylcyclobutan-1,3-dione.

Sources & evidence

ORD record: ord-5cd6d19a6a4b457a8c595d50914ae212
Source dataset: uspto-grants-1977_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04048423

Reaction notes

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