HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 4-(2-Nitro-4-(trifluoromethyl)phenyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 4-Chloro-alpha,alpha,alpha-trifluoro-3-nitrotoluene | HCID 8462 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 4-(2-Nitro-4-(trifluoromethyl)phenyl)morpholine | HCID 2775793 | — |
Reaction Steps
4(2-Nitro-4-trifluoromethylphenyl)morpholine was prepared by reaction of 4-chloro-3-nitrobenzotrifluoride with equimolar amounts of morpholine and triethylamine in monoglyme. The resultant product melts at 37° - 39° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049422 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-545d1afadd0c485b99f7bbdcf2a1c301 |
| Source note | uspto-grants-1977_09 |