HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzaldehyde → HCID 70631684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzaldehyde | HCID 11101 | — |
| Reactant | Carbamimidoyl-acetic acid ethyl ester | HCID 4599837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70631684 | HCID 70631684 | 56% |
Reaction Steps
Upon boiling a solution of 7.6 g 2-nitrobenzaldehyde and 13.0 g amidinoacetic acid ethyl ester in 150 ml ethanol for 2 hours, 2,6-diamino-4-(2-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester of m.p. 142° C. (ethanol) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049662 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-46da897f1a584cf18db301d9c6e7af0a |
| Source note | uspto-grants-1977_09 |