HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 21409949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | N-[2-Methylamino-2-methylpropyl]benzamide | HCID 21409819 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 21409949 | HCID 21409949 | — |
Reaction Steps
A solution of N-[2-methylamino-2-methylpropyl]benzamide (1. g.,) in MEK (25 ml.) was added to a solution of allyl bromide (0.58 g.,) in MEK (25 ml.) containing sodium carbonate (0.55 g.,) and a few crystals of sodium iodide. The mixture was refluxed for 24 hrs. The inorganic solids were filtered off and the filtrant concentrated by evaporation under reduced pressure. The liquid residue was eluted down an alumina column with ethyl acetate to give N-[2-(allylmethylamino)-2-methylpropyl]benzamide 1.1 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049663 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-bb395d98b9364963be2b85640abfca96 |
| Source note | uspto-grants-1977_09 |