HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70600924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 70600837 | HCID 70600837 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 70600924 | HCID 70600924 | — |
Reaction Steps
2.56 g. of 1-methoxy-3-p-biphenylyl-3-butanol (obtainable from 3-methoxy-1-p-biphenylyl-1-propanone and CH3MgI) is boiled for 2 hours with a mixture of 5 ml. of 48% aqueous HBr and 5 ml. of acetic acid, 10 ml. of 10% methanolic KOH are added and boiling is continued for a further 2 hours and the mixture is worked up using water and chloroform to give 3-p-biphenylyl-1,3-butanediol, m.p. 115°-117°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049823 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-f9838adb5ad341599d5d8a906db53cf8 |
| Source note | uspto-grants-1977_09 |