HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 2-[(2-Fluorophenyl)methanesulfinyl]-1-oxo-1lambda~5~-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 45692353 | HCID 45692353 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-[(2-Fluorophenyl)methanesulfinyl]-1-oxo-1lambda~5~-pyridine | HCID 54013755 | — |
Reaction Steps
The procedure employed is identical to that of Example 68 using 5.7 gm (0.024 mol) 2-(2-fluorophenylmethylthio)pyridine N-oxide in 50 ml of chloroform with 4.8 gm (0.024 mol) MCPBA in 75 ml chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04050921 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-d810f712ebb348dcb4892b3ef5115267 |
| Source note | uspto-grants-1977_09 |