HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 4-[(1-Oxo-1lambda~5~-pyridine-2-sulfinyl)methyl]benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 8605527 | HCID 8605527 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-[(1-Oxo-1lambda~5~-pyridine-2-sulfinyl)methyl]benzonitrile | HCID 54404939 | — |
Reaction Steps
The procedure employed is identical to that of Example 68 using 3.6 gm (0.015 mol) 2-(4-cyanophenylmethylthio)pyridine N-oxide in 50 ml of chloroform with 3 gm (0.015 mol) MCPBA in 50 ml chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04050921 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-8dcdfe66678d4a8d90a30b82575a0c29 |
| Source note | uspto-grants-1977_09 |