HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 2-[(2,4-Dichlorophenyl)methanesulfinyl]-1-oxo-1lambda~5~-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 2-{[(2,4-Dichlorophenyl)methyl]sulfanyl}-1-oxo-1lambda~5~-pyridine | HCID 47095502 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-[(2,4-Dichlorophenyl)methanesulfinyl]-1-oxo-1lambda~5~-pyridine | HCID 54493254 | — |
Reaction Steps
The procedure employed is identical to that of Example 68 using 5.8 gm (0.02 mol) 2-(2,4-Dichlorophenylmethylthio)pyridine N-oxide in 50 ml of chloroform and 4 gm (0.02 mol) MCPBA in 100 ml of chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04050921 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-fe3605e4d17941eb8057845727cce031 |
| Source note | uspto-grants-1977_09 |